Ruthenium Ion-Catalyzed Oxidation of Shenfu Coal and Its Residues
Shenfu coal (SFC), its liquefaction residue (RL), and carbon disulfide (CS2)/tetrahydrofuran (THF)-inextractable matter (RE) were subject to ruthenium ion-catalyzed oxidation to understand the differences in structural features among the above three samples. The results suggest that SFC is rich in l...
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| Published in | Energy & fuels Vol. 22; no. 3; pp. 1799 - 1806 |
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| Main Authors | , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Washington, DC
American Chemical Society
01.05.2008
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| Abstract | Shenfu coal (SFC), its liquefaction residue (RL), and carbon disulfide (CS2)/tetrahydrofuran (THF)-inextractable matter (RE) were subject to ruthenium ion-catalyzed oxidation to understand the differences in structural features among the above three samples. The results suggest that SFC is rich in long-chain arylalkanes and α,ω-diarylalkanes (DAAs) with carbon number of methylene linkage from 2 to 4 and that long-chain arylalkanes and DAAs are reactive toward hydroliquefaction and soluble in a CS2/THF mixed solvent, whereas highly condensed aromatic species in SFC show poor solubility in the CS2/THF mixed solvent. |
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| AbstractList | Shenfu coal (SFC), its liquefaction residue (RL), and carbon disulfide (CS2)/tetrahydrofuran (THF)-inextractable matter (RE) were subject to ruthenium ion-catalyzed oxidation to understand the differences in structural features among the above three samples. The results suggest that SFC is rich in long-chain arylalkanes and α,ω-diarylalkanes (DAAs) with carbon number of methylene linkage from 2 to 4 and that long-chain arylalkanes and DAAs are reactive toward hydroliquefaction and soluble in a CS2/THF mixed solvent, whereas highly condensed aromatic species in SFC show poor solubility in the CS2/THF mixed solvent. Shenfu coal (SFC), its liquefaction residue (RL), and carbon disulfide (CS{sub 2})/tetrahydrofuran (THF)-inextractable matter (RE) were subject to ruthenium ion-catalyzed oxidation to understand the differences in structural features among the above three samples. The results suggest that SFC is rich in long-chain arylalkanes and {alpha}. {omega}-diarylalkanes (DAAs) with carbon number of methylene linkage from 2 to 4 and that long-chain arylalkanes and DAAs are reactive toward hydroliquefaction and soluble in a CS{sub 2}/THF mixed solvent, whereas highly condensed aromatic species in SFC show poor solubility in the CS{sub 2}/THF mixed solvent. 29 refs., 6 figs., 4 tabs. |
| Author | Zhao, Wei Cai, Ke-Ying Zong, Zhi-Min Ding, Ming-Jie Wei, Xian-Yong Zheng, Yu-Xuan Mou, Jie Wang, Feng Huang, Yao-Guo Cao, Jin-Pei Yao, Zi-Shuo Liu, Guang-Feng Xia, Zhi-Lin Wu, Lin |
| Author_xml | – sequence: 1 givenname: Yao-Guo surname: Huang fullname: Huang, Yao-Guo – sequence: 2 givenname: Zhi-Min surname: Zong fullname: Zong, Zhi-Min – sequence: 3 givenname: Zi-Shuo surname: Yao fullname: Yao, Zi-Shuo – sequence: 4 givenname: Yu-Xuan surname: Zheng fullname: Zheng, Yu-Xuan – sequence: 5 givenname: Jie surname: Mou fullname: Mou, Jie – sequence: 6 givenname: Guang-Feng surname: Liu fullname: Liu, Guang-Feng – sequence: 7 givenname: Jin-Pei surname: Cao fullname: Cao, Jin-Pei – sequence: 8 givenname: Ming-Jie surname: Ding fullname: Ding, Ming-Jie – sequence: 9 givenname: Ke-Ying surname: Cai fullname: Cai, Ke-Ying – sequence: 10 givenname: Feng surname: Wang fullname: Wang, Feng – sequence: 11 givenname: Wei surname: Zhao fullname: Zhao, Wei – sequence: 12 givenname: Zhi-Lin surname: Xia fullname: Xia, Zhi-Lin – sequence: 13 givenname: Lin surname: Wu fullname: Wu, Lin – sequence: 14 givenname: Xian-Yong surname: Wei fullname: Wei, Xian-Yong email: wei_xianyong@163.com |
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| Keywords | Mixed solvent Liquefaction Solubility Oxidation Hydroliquefaction Bituminous coal Ruthenium ion |
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| Notes | Mass spectra of methylated products from MCAs, DCAs, TCAs, CCAs, and BCAs in Supporting Information I along with the extraction procedure of SFC and data from soluble fractions of SFC in Supporting Information II. This material is available free of charge via the Internet at http://pubs.acs.org. ark:/67375/TPS-X34LTHDW-B istex:E0DC15AF3E87426F8DCE51C110900232BEF927EA |
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| Snippet | Shenfu coal (SFC), its liquefaction residue (RL), and carbon disulfide (CS2)/tetrahydrofuran (THF)-inextractable matter (RE) were subject to ruthenium... Shenfu coal (SFC), its liquefaction residue (RL), and carbon disulfide (CS{sub 2})/tetrahydrofuran (THF)-inextractable matter (RE) were subject to ruthenium... |
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| SubjectTerms | 01 COAL, LIGNITE, AND PEAT Applied sciences CATALYSIS COAL COAL LIQUEFACTION Energy Exact sciences and technology Fossil Fuels Fuel processing. Carbochemistry and petrochemistry Fuels MOLECULAR STRUCTURE OXIDATION RESIDUES RUTHENIUM Solid fuel processing (coal, coke, brown coal, peat, wood, etc.) STRUCTURAL CHEMICAL ANALYSIS |
| Title | Ruthenium Ion-Catalyzed Oxidation of Shenfu Coal and Its Residues |
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