Unusual Li+ Ion Solvation Structure in Bis(fluorosulfonyl)amide Based Ionic Liquid
Raman spectra of 1-ethyl-3-methylimidazolium bis(fluorosulfonyl)amide [C2mIm+][FSA–] ionic liquid solutions dissolving LiFSA salt of various concentrations were measured at 298 K. FSA– ((FSO2)2N–) is an analogue anion of bis(trifluoromethanesulfonyl)amide ((CF3SO2)2N–; TFSA–). We found that a solvat...
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Published in | Journal of physical chemistry. C Vol. 117; no. 38; pp. 19314 - 19324 |
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Main Authors | , , , , , , , , , , |
Format | Journal Article |
Language | English |
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Columbus, OH
American Chemical Society
26.09.2013
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Abstract | Raman spectra of 1-ethyl-3-methylimidazolium bis(fluorosulfonyl)amide [C2mIm+][FSA–] ionic liquid solutions dissolving LiFSA salt of various concentrations were measured at 298 K. FSA– ((FSO2)2N–) is an analogue anion of bis(trifluoromethanesulfonyl)amide ((CF3SO2)2N–; TFSA–). We found that a solvation number of the Li+ ion in [C2mIm+][FSA–] is 3, though it has been well established that Li+ ion is solvated by two TFSA– anions in the corresponding ionic liquids below the Li+ ion mole fraction of x Li+ < 0.2. To yield further insight into larger solvation numbers, Raman spectra were measured at higher temperatures up to 364 K. The Li+ ion solvation number in [C2mIm+][FSA–] evidently decreased when the temperature was elevated. Temperature dependence of the Li+ ion solvation number was analyzed assuming an equilibrium between [Li(FSA)2]− and [Li(FSA)3]2–, and the enthalpy ΔH° and the temperature multiplied entropy TΔS° for one FSA– liberation toward a bulk ionic liquid were successfully evaluated to be 35(2) kJ mol–1 and 29(2) kJ mol–1, respectively. The ΔH° and ΔS° suggest that the Li+ ion is coordinated by one of bidentate and two of monodentate FSA– at 298 K, and that the more weakly solvated monodentate FSA– is liberated at higher temperatures. The high-energy X-ray diffraction (HEXRD) experiments of these systems were carried out and were analyzed with the aid of molecular dynamics (MD) simulations. In radial distribution functions evaluated with HEXRD, a peak at about 1.94 Å appeared and was attributable to the Li+–O(FSA–) correlations. The longer Li+–O(FSA–) distance than that for the Li+–O(TFSA–) of 1.86 Å strongly supports the larger solvation number of the Li+ ions in the FSA– based ionic liquids. MD simulations at least qualitatively reproduced the Raman and HEXRD experiments. |
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AbstractList | Raman spectra of 1-ethyl-3-methylimidazolium bis(fluorosulfonyl)amide [C2mIm+][FSA–] ionic liquid solutions dissolving LiFSA salt of various concentrations were measured at 298 K. FSA– ((FSO2)2N–) is an analogue anion of bis(trifluoromethanesulfonyl)amide ((CF3SO2)2N–; TFSA–). We found that a solvation number of the Li+ ion in [C2mIm+][FSA–] is 3, though it has been well established that Li+ ion is solvated by two TFSA– anions in the corresponding ionic liquids below the Li+ ion mole fraction of x Li+ < 0.2. To yield further insight into larger solvation numbers, Raman spectra were measured at higher temperatures up to 364 K. The Li+ ion solvation number in [C2mIm+][FSA–] evidently decreased when the temperature was elevated. Temperature dependence of the Li+ ion solvation number was analyzed assuming an equilibrium between [Li(FSA)2]− and [Li(FSA)3]2–, and the enthalpy ΔH° and the temperature multiplied entropy TΔS° for one FSA– liberation toward a bulk ionic liquid were successfully evaluated to be 35(2) kJ mol–1 and 29(2) kJ mol–1, respectively. The ΔH° and ΔS° suggest that the Li+ ion is coordinated by one of bidentate and two of monodentate FSA– at 298 K, and that the more weakly solvated monodentate FSA– is liberated at higher temperatures. The high-energy X-ray diffraction (HEXRD) experiments of these systems were carried out and were analyzed with the aid of molecular dynamics (MD) simulations. In radial distribution functions evaluated with HEXRD, a peak at about 1.94 Å appeared and was attributable to the Li+–O(FSA–) correlations. The longer Li+–O(FSA–) distance than that for the Li+–O(TFSA–) of 1.86 Å strongly supports the larger solvation number of the Li+ ions in the FSA– based ionic liquids. MD simulations at least qualitatively reproduced the Raman and HEXRD experiments. |
Author | Dokko, Kaoru Hamano, Hiroshi Hayamizu, Kikuko Watanabe, Masayoshi Doi, Hiroyuki Tsuzuki, Seiji Seki, Shiro Umebayashi, Yasuhiro Kameda, Yasuo Song, Xuedan Fujii, Kenta |
AuthorAffiliation | Neutron Science Labolatory, Institute for Solid State Physics Yamagata University Department of Chemistry and Biotechnology Kyushu University Department of Chemistry, Faculty of Science National Institute of Advanced Industrial Science and Technology (AIST) The University of Tokyo Materials Science Research Laboratory Central Research Institute of Electric Power Industry Yokohama National University Graduate School of Science and Technology Niigata University State Key Laboratory of Fine Chemicals Dalian University of Technology Department of Material and Biological Chemistry, Faculty of Science |
AuthorAffiliation_xml | – name: The University of Tokyo – name: Kyushu University – name: Materials Science Research Laboratory – name: Graduate School of Science and Technology – name: Yokohama National University – name: Department of Material and Biological Chemistry, Faculty of Science – name: National Institute of Advanced Industrial Science and Technology (AIST) – name: Neutron Science Labolatory, Institute for Solid State Physics – name: State Key Laboratory of Fine Chemicals – name: Yamagata University – name: Central Research Institute of Electric Power Industry – name: Department of Chemistry, Faculty of Science – name: Department of Chemistry and Biotechnology – name: Niigata University – name: Dalian University of Technology |
Author_xml | – sequence: 1 givenname: Kenta surname: Fujii fullname: Fujii, Kenta – sequence: 2 givenname: Hiroshi surname: Hamano fullname: Hamano, Hiroshi – sequence: 3 givenname: Hiroyuki surname: Doi fullname: Doi, Hiroyuki – sequence: 4 givenname: Xuedan surname: Song fullname: Song, Xuedan – sequence: 5 givenname: Seiji surname: Tsuzuki fullname: Tsuzuki, Seiji email: s.tsuzuki@aist.go.jp – sequence: 6 givenname: Kikuko surname: Hayamizu fullname: Hayamizu, Kikuko – sequence: 7 givenname: Shiro surname: Seki fullname: Seki, Shiro – sequence: 8 givenname: Yasuo surname: Kameda fullname: Kameda, Yasuo – sequence: 9 givenname: Kaoru surname: Dokko fullname: Dokko, Kaoru – sequence: 10 givenname: Masayoshi surname: Watanabe fullname: Watanabe, Masayoshi – sequence: 11 givenname: Yasuhiro surname: Umebayashi fullname: Umebayashi, Yasuhiro email: yumescc@chem.sc.niigata-u.ac.jp |
BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=27784073$$DView record in Pascal Francis |
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Keywords | Temperature dependence Raman spectra Enthalpy Molecular dynamics method Theoretical study Amides Entropy XRD Raman spectroscopy Solvation High energy Radial distribution function Thermodynamic properties |
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Snippet | Raman spectra of 1-ethyl-3-methylimidazolium bis(fluorosulfonyl)amide [C2mIm+][FSA–] ionic liquid solutions dissolving LiFSA salt of various concentrations... |
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SubjectTerms | Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Physics Thermal properties of condensed matter Thermal properties of crystalline solids Thermodynamic properties |
Title | Unusual Li+ Ion Solvation Structure in Bis(fluorosulfonyl)amide Based Ionic Liquid |
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