Adsorption and Diffusion of Benzene on Chromium-Based Metal Organic Framework MIL-101 Synthesized by Microwave Irradiation
Adsorption equilibrium and diffusion of benzene on mesoporous chromium−terphthalate-based crystals (MIL-101) were experimentally studied by the gravimetric method in the pressure range up to 60.0 mbar. The MIL-101 crystals, whose sizes are about 100 nm, were synthesized by using microwave irradiatio...
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| Published in | Industrial & engineering chemistry research Vol. 50; no. 4; pp. 2254 - 2261 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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American Chemical Society
16.02.2011
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| Abstract | Adsorption equilibrium and diffusion of benzene on mesoporous chromium−terphthalate-based crystals (MIL-101) were experimentally studied by the gravimetric method in the pressure range up to 60.0 mbar. The MIL-101 crystals, whose sizes are about 100 nm, were synthesized by using microwave irradiation method. Adsorption isotherms and kinetic curves of benzene on the MIL-101 were measured experimentally. Results show that the maximum amount adsorbed of benzene on the synthesized MIL-101 was up to 16.5 mmol/g (or 176 wt %) at 288 K and 56.0 mbar. Diffusion coefficients of benzene within the MIL-101 were in the range of (4.25−4.76) × 10−9 cm2/s in 288−318 K with a lower activation energy of 2.41 kJ/mol. Temperature programmed desorption (TPD) curves exhibited two separated peaks corresponding to two types of major adsorption sites for benzene adsorption on MIL-101. Consecutive cycles of adsorption−desorption experiment showed a fast desorption kinetics and high reversibility for benzene adsorption on MIL-101. The efficiency of benzene desorption from MIL-101 can reach 97%. |
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| AbstractList | Adsorption equilibrium and diffusion of benzene on mesoporous chromium−terphthalate-based crystals (MIL-101) were experimentally studied by the gravimetric method in the pressure range up to 60.0 mbar. The MIL-101 crystals, whose sizes are about 100 nm, were synthesized by using microwave irradiation method. Adsorption isotherms and kinetic curves of benzene on the MIL-101 were measured experimentally. Results show that the maximum amount adsorbed of benzene on the synthesized MIL-101 was up to 16.5 mmol/g (or 176 wt %) at 288 K and 56.0 mbar. Diffusion coefficients of benzene within the MIL-101 were in the range of (4.25−4.76) × 10−9 cm2/s in 288−318 K with a lower activation energy of 2.41 kJ/mol. Temperature programmed desorption (TPD) curves exhibited two separated peaks corresponding to two types of major adsorption sites for benzene adsorption on MIL-101. Consecutive cycles of adsorption−desorption experiment showed a fast desorption kinetics and high reversibility for benzene adsorption on MIL-101. The efficiency of benzene desorption from MIL-101 can reach 97%. |
| Author | Xia, Qibin Zhao, Zhenxia Li, Xuemei Huang, Sisi Li, Zhong |
| AuthorAffiliation | South China University of Technology School of Materials Science and Engineering School of Chemistry and Chemical Engineering State Key Laboratory of Subtropical Building Science |
| AuthorAffiliation_xml | – name: South China University of Technology – name: School of Chemistry and Chemical Engineering – name: State Key Laboratory of Subtropical Building Science – name: School of Materials Science and Engineering |
| Author_xml | – sequence: 1 givenname: Zhenxia surname: Zhao fullname: Zhao, Zhenxia – sequence: 2 givenname: Xuemei surname: Li fullname: Li, Xuemei – sequence: 3 givenname: Sisi surname: Huang fullname: Huang, Sisi – sequence: 4 givenname: Qibin surname: Xia fullname: Xia, Qibin – sequence: 5 givenname: Zhong surname: Li fullname: Li, Zhong email: cezhli@scut.edu.cn |
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| SubjectTerms | Adsorption Applied sciences Chemical engineering Exact sciences and technology Separations |
| Title | Adsorption and Diffusion of Benzene on Chromium-Based Metal Organic Framework MIL-101 Synthesized by Microwave Irradiation |
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