The Covalent and Coordination Co-Driven Assembly of Supramolecular Octahedral Cages with Controllable Degree of Distortion

Discovering and constructing novel and fancy structures is the goal of many supramolecular chemists. In this work, we propose an assembly strategy based on the synergistic effect of coordination and covalent interactions to construct a set of octahedral supramolecular cages and adjust their degree o...

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Published inJournal of the American Chemical Society Vol. 142; no. 31; pp. 13356 - 13361
Main Authors Bao, Shu-Jin, Xu, Ze-Ming, Ju, Yun, Song, Ying-Lin, Wang, Heng, Niu, Zheng, Li, Xiaopeng, Braunstein, Pierre, Lang, Jian-Ping
Format Journal Article
LanguageEnglish
Published American Chemical Society 05.08.2020
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Chemical Sciences
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Abstract Discovering and constructing novel and fancy structures is the goal of many supramolecular chemists. In this work, we propose an assembly strategy based on the synergistic effect of coordination and covalent interactions to construct a set of octahedral supramolecular cages and adjust their degree of distortion. Our strategy innovatively utilizes the addition of sulfur atoms of a metal sulfide synthon, [Et4N]­[Tp*WS3] (A), to an alkynyl group of a pyridine-containing linker, resulting in a novel vertex with low symmetry, and of Cu­(I) ions. By adjusting the length of the linker and the position of the reactive alkynyl group, the control of the deformation degree of the octahedral cages can be realized. These supramolecular cages exhibit enhanced third-order nonlinear optical (NLO) responses. The results offer a powerful strategy to construct novel distorted cage structures as well as control the degree of distortion of supramolecular geometries.
AbstractList Discovering and constructing novel and fancy structures is the goal of many supramolecular chemists. In this work, we propose an assembly strategy based on the synergistic effect of coordination and covalent interactions to construct a set of octahedral supramolecular cages and adjust their degree of distortion. Our strategy innovatively utilizes the addition of sulfur atoms of a metal sulfide synthon, [Et4N]­[Tp*WS3] (A), to an alkynyl group of a pyridine-containing linker, resulting in a novel vertex with low symmetry, and of Cu­(I) ions. By adjusting the length of the linker and the position of the reactive alkynyl group, the control of the deformation degree of the octahedral cages can be realized. These supramolecular cages exhibit enhanced third-order nonlinear optical (NLO) responses. The results offer a powerful strategy to construct novel distorted cage structures as well as control the degree of distortion of supramolecular geometries.
Author Braunstein, Pierre
Ju, Yun
Lang, Jian-Ping
Bao, Shu-Jin
Xu, Ze-Ming
Li, Xiaopeng
Wang, Heng
Song, Ying-Lin
Niu, Zheng
AuthorAffiliation Chemistry Department
Soochow University
Institut de Chimie (UMR 7177 CNRS)
School of Physical Science and Technology
Université de Strasbourg
Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences
State Key Laboratory of Organometallic Chemistry
College of Chemistry, Chemical Engineering and Materials Science
AuthorAffiliation_xml – name: Soochow University
– name: School of Physical Science and Technology
– name: Chemistry Department
– name: Université de Strasbourg
– name: Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences
– name: Institut de Chimie (UMR 7177 CNRS)
– name: State Key Laboratory of Organometallic Chemistry
– name: College of Chemistry, Chemical Engineering and Materials Science
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  fullname: Bao, Shu-Jin
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  organization: Université de Strasbourg
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  orcidid: 0000-0003-2942-7385
  surname: Lang
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  email: jplang@suda.edu.cn
  organization: Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences
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Snippet Discovering and constructing novel and fancy structures is the goal of many supramolecular chemists. In this work, we propose an assembly strategy based on the...
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Title The Covalent and Coordination Co-Driven Assembly of Supramolecular Octahedral Cages with Controllable Degree of Distortion
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