Influence of Hydrogen Bonding on Photopolymerization Rate of Hydroxyalkyl Acrylates

The relationship between the photopolymerization rate of hydroxyalkyl acrylates and their structure has been investigated. The polymerization rates of hydroxyalkyl acrylates are significantly higher than those observed for typical monofunctional acrylate monomers and rival those of multifunctional m...

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Published inMacromolecules Vol. 37; no. 10; pp. 3659 - 3665
Main Authors Lee, Tai Y, Roper, Todd M, Jönsson, E. Sonny, Guymon, C. A, Hoyle, C. E
Format Journal Article
LanguageEnglish
Published Washington, DC American Chemical Society 18.05.2004
Subjects
Applied sciences
Exact sciences and technology
Physicochemistry of polymers
Polymerization
Polymers and radiations
Substituent effect
Bulk polymerization
Experimental study
Reaction rate
Alcohol polymer
Acrylate polymer
Photopolymerization
Hydroxyethyl acrylate polymer
Kinetics
Monomer
Chemical reactivity
Activation energy
Alkyl acrylate polymer
Hydrogen bond
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Abstract The relationship between the photopolymerization rate of hydroxyalkyl acrylates and their structure has been investigated. The polymerization rates of hydroxyalkyl acrylates are significantly higher than those observed for typical monofunctional acrylate monomers and rival those of multifunctional monomers. By polymerizing at several temperatures, it was shown that the enhanced rates are directly proportional to the degree of hydrogen bonding. Apparently, termination rates are greatly reduced by hydrogen bonding, which is present in both the unpolymerized monomer and the final polymer film.
AbstractList The relationship between the photopolymerization rate of hydroxyalkyl acrylates and their structure has been investigated. The polymerization rates of hydroxyalkyl acrylates are significantly higher than those observed for typical monofunctional acrylate monomers and rival those of multifunctional monomers. By polymerizing at several temperatures, it was shown that the enhanced rates are directly proportional to the degree of hydrogen bonding. Apparently, termination rates are greatly reduced by hydrogen bonding, which is present in both the unpolymerized monomer and the final polymer film.
Author Jönsson, E. Sonny
Roper, Todd M
Hoyle, C. E
Guymon, C. A
Lee, Tai Y
Author_xml – sequence: 1
  givenname: Tai Y
  surname: Lee
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  givenname: Todd M
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  givenname: E. Sonny
  surname: Jönsson
  fullname: Jönsson, E. Sonny
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  givenname: C. A
  surname: Guymon
  fullname: Guymon, C. A
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  givenname: C. E
  surname: Hoyle
  fullname: Hoyle, C. E
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Issue 10
Keywords Substituent effect
Bulk polymerization
Experimental study
Reaction rate
Alcohol polymer
Acrylate polymer
Photopolymerization
Hydroxyethyl acrylate polymer
Kinetics
Monomer
Chemical reactivity
Activation energy
Alkyl acrylate polymer
Hydrogen bond
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Snippet The relationship between the photopolymerization rate of hydroxyalkyl acrylates and their structure has been investigated. The polymerization rates of...
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SubjectTerms Applied sciences
Exact sciences and technology
Physicochemistry of polymers
Polymerization
Polymers and radiations
Title Influence of Hydrogen Bonding on Photopolymerization Rate of Hydroxyalkyl Acrylates
URI http://dx.doi.org/10.1021/ma0305277
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