Introducing Frustrated Lewis Pairs to Metal–Organic Framework for Selective Hydrogenation of N‑Heterocycles
Hydrogenated nitrogen heterocyclic compounds play a critical role in the pharmaceutical, polymer, and agrochemical industries. Recent studies on partial hydrogenation of nitrogen heterocyclic compounds have focused on costly and toxic precious metal catalysts. As an important class of main-group cat...
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Published in | Journal of the American Chemical Society Vol. 145; no. 27; pp. 14994 - 15000 |
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Main Authors | , , , , , , , , |
Format | Journal Article |
Language | English |
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12.07.2023
Amer Chemical Soc |
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Abstract | Hydrogenated nitrogen heterocyclic compounds play a critical role in the pharmaceutical, polymer, and agrochemical industries. Recent studies on partial hydrogenation of nitrogen heterocyclic compounds have focused on costly and toxic precious metal catalysts. As an important class of main-group catalysts, frustrated Lewis pairs (FLPs) have been widely applied in catalytic hydrogenation reactions. In principle, the combination of FLPs and metal–organic framework (MOF) is anticipated to efficiently enhance the recyclability performance of FLPs; however, the previously studied MOF-FLPs showed low reactivity in the hydrogenation of N-heterocycles compounds. Herein, we offer a novel P/B type MOF-FLP catalyst that was achieved via a solvent-assisted linker incorporation approach to boost catalytic hydrogenation reactions. Using hydrogen gas under moderate pressure, the proposed P/B type MOF-FLP can serve as a highly efficient heterogeneous catalyst for selective hydrogenation of quinoline and indole to tetrahydroquinoline and indoline-type drug compounds in high yield and excellent recyclability. |
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AbstractList | Hydrogenated nitrogen heterocyclic compounds play a critical role in the pharmaceutical, polymer, and agrochemical industries. Recent studies on partial hydrogenation of nitrogen heterocyclic compounds have focused on costly and toxic precious metal catalysts. As an important class of main-group catalysts, frustrated Lewis pairs (FLPs) have been widely applied in catalytic hydrogenation reactions. In principle, the combination of FLPs and metal-organic framework (MOF) is anticipated to efficiently enhance the recyclability performance of FLPs; however, the previously studied MOF-FLPs showed low reactivity in the hydrogenation of
-heterocycles compounds. Herein, we offer a novel P/B type MOF-FLP catalyst that was achieved via a solvent-assisted linker incorporation approach to boost catalytic hydrogenation reactions. Using hydrogen gas under moderate pressure, the proposed P/B type MOF-FLP can serve as a highly efficient heterogeneous catalyst for selective hydrogenation of quinoline and indole to tetrahydroquinoline and indoline-type drug compounds in high yield and excellent recyclability. Hydrogenated nitrogen heterocyclic compounds play a criticalrolein the pharmaceutical, polymer, and agrochemical industries. Recentstudies on partial hydrogenation of nitrogen heterocyclic compoundshave focused on costly and toxic precious metal catalysts. As an importantclass of main-group catalysts, frustrated Lewis pairs (FLPs) havebeen widely applied in catalytic hydrogenation reactions. In principle,the combination of FLPs and metal-organic framework (MOF) isanticipated to efficiently enhance the recyclability performance ofFLPs; however, the previously studied MOF-FLPs showed low reactivityin the hydrogenation of N-heterocycles compounds.Herein, we offer a novel P/B type MOF-FLP catalyst that was achievedvia a solvent-assisted linker incorporation approach to boost catalytichydrogenation reactions. Using hydrogen gas under moderate pressure,the proposed P/B type MOF-FLP can serve as a highly efficient heterogeneouscatalyst for selective hydrogenation of quinoline and indole to tetrahydroquinolineand indoline-type drug compounds in high yield and excellent recyclability. Hydrogenated nitrogen heterocyclic compounds play a critical role in the pharmaceutical, polymer, and agrochemical industries. Recent studies on partial hydrogenation of nitrogen heterocyclic compounds have focused on costly and toxic precious metal catalysts. As an important class of main-group catalysts, frustrated Lewis pairs (FLPs) have been widely applied in catalytic hydrogenation reactions. In principle, the combination of FLPs and metal–organic framework (MOF) is anticipated to efficiently enhance the recyclability performance of FLPs; however, the previously studied MOF-FLPs showed low reactivity in the hydrogenation of N-heterocycles compounds. Herein, we offer a novel P/B type MOF-FLP catalyst that was achieved via a solvent-assisted linker incorporation approach to boost catalytic hydrogenation reactions. Using hydrogen gas under moderate pressure, the proposed P/B type MOF-FLP can serve as a highly efficient heterogeneous catalyst for selective hydrogenation of quinoline and indole to tetrahydroquinoline and indoline-type drug compounds in high yield and excellent recyclability. |
Author | Huang, Yali Lang, Jian-Ping Bao, Shu-Jin Hu, Zhuoyi Xu, Ze-Ming Nafady, Ayman Al-Enizi, Abdullah M. Ma, Shengqian Niu, Zheng |
AuthorAffiliation | Department of Chemistry Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences Department of Chemistry, College of Science State Key Laboratory of Organometallic Chemistry College of Chemistry, Chemical Engineering and Materials Science |
AuthorAffiliation_xml | – name: Department of Chemistry – name: Department of Chemistry, College of Science – name: State Key Laboratory of Organometallic Chemistry – name: College of Chemistry, Chemical Engineering and Materials Science – name: Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences |
Author_xml | – sequence: 1 givenname: Ze-Ming surname: Xu fullname: Xu, Ze-Ming organization: College of Chemistry, Chemical Engineering and Materials Science – sequence: 2 givenname: Zhuoyi surname: Hu fullname: Hu, Zhuoyi organization: College of Chemistry, Chemical Engineering and Materials Science – sequence: 3 givenname: Yali surname: Huang fullname: Huang, Yali organization: College of Chemistry, Chemical Engineering and Materials Science – sequence: 4 givenname: Shu-Jin surname: Bao fullname: Bao, Shu-Jin organization: College of Chemistry, Chemical Engineering and Materials Science – sequence: 5 givenname: Zheng orcidid: 0000-0003-2406-997X surname: Niu fullname: Niu, Zheng email: zhengniu@suda.edu.cn organization: College of Chemistry, Chemical Engineering and Materials Science – sequence: 6 givenname: Jian-Ping orcidid: 0000-0003-2942-7385 surname: Lang fullname: Lang, Jian-Ping email: jplang@suda.edu.cn organization: Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences – sequence: 7 givenname: Abdullah M. orcidid: 0000-0002-3967-5553 surname: Al-Enizi fullname: Al-Enizi, Abdullah M. organization: Department of Chemistry, College of Science – sequence: 8 givenname: Ayman surname: Nafady fullname: Nafady, Ayman organization: Department of Chemistry, College of Science – sequence: 9 givenname: Shengqian orcidid: 0000-0002-1897-7069 surname: Ma fullname: Ma, Shengqian email: Shengqian.Ma@unt.edu organization: Department of Chemistry |
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SSID | ssj0004281 |
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Snippet | Hydrogenated nitrogen heterocyclic compounds play a critical role in the pharmaceutical, polymer, and agrochemical industries. Recent studies on partial... Hydrogenated nitrogen heterocyclic compounds play a criticalrolein the pharmaceutical, polymer, and agrochemical industries. Recentstudies on partial... |
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SubjectTerms | Chemistry Chemistry, Multidisciplinary Physical Sciences Science & Technology |
Title | Introducing Frustrated Lewis Pairs to Metal–Organic Framework for Selective Hydrogenation of N‑Heterocycles |
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