In Situ Environmental Transmission Electron Microscopy Investigation on LiH Formation Prompted by LiF
Lithium hydride is a common but unfavorable component that leads to “dead Li” formation in lithium batteries. Since the hydrogen sources in the batteries are diverse and hardly evitable, unraveling the key factors promoting LiH formation is fundamentally crucial in improving lithium batteries’ cycli...
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| Published in | Nano letters Vol. 25; no. 20; pp. 8303 - 8309 |
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| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
21.05.2025
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| Abstract | Lithium hydride is a common but unfavorable component that leads to “dead Li” formation in lithium batteries. Since the hydrogen sources in the batteries are diverse and hardly evitable, unraveling the key factors promoting LiH formation is fundamentally crucial in improving lithium batteries’ cycling stability. Herein, by using in situ environmental transmission electron microscope, we revealed a critical role of lithium fluoride in the LiH formation during the electrochemical deposition of Li in a hydrogen environment, presumably by facilitating the kinetic process of hydrogen dissociation and the LiH nucleation. Ex situ coin-cell studies and DFT calculations corroborate this finding, further suggesting that the commonly used fluorine-rich electrolytes could promote LiH formation. Additionally, the LiH lattices in the dendrites are distorted and likely nonstoichiometric with face-centered cubic structured domains of Li metal. These fundamental insights on the LiH formation may pave the way for enhancing the cycle stability of lithium batteries. |
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| AbstractList | Lithium hydride is a common but unfavorable component that leads to "dead Li" formation in lithium batteries. Since the hydrogen sources in the batteries are diverse and hardly evitable, unraveling the key factors promoting LiH formation is fundamentally crucial in improving lithium batteries' cycling stability. Herein, by using
environmental transmission electron microscope, we revealed a critical role of lithium fluoride in the LiH formation during the electrochemical deposition of Li in a hydrogen environment, presumably by facilitating the kinetic process of hydrogen dissociation and the LiH nucleation.
coin-cell studies and DFT calculations corroborate this finding, further suggesting that the commonly used fluorine-rich electrolytes could promote LiH formation. Additionally, the LiH lattices in the dendrites are distorted and likely nonstoichiometric with face-centered cubic structured domains of Li metal. These fundamental insights on the LiH formation may pave the way for enhancing the cycle stability of lithium batteries. Lithium hydride is a common but unfavorable component that leads to "dead Li" formation in lithium batteries. Since the hydrogen sources in the batteries are diverse and hardly evitable, unraveling the key factors promoting LiH formation is fundamentally crucial in improving lithium batteries' cycling stability. Herein, by using in situ environmental transmission electron microscope, we revealed a critical role of lithium fluoride in the LiH formation during the electrochemical deposition of Li in a hydrogen environment, presumably by facilitating the kinetic process of hydrogen dissociation and the LiH nucleation. Ex situ coin-cell studies and DFT calculations corroborate this finding, further suggesting that the commonly used fluorine-rich electrolytes could promote LiH formation. Additionally, the LiH lattices in the dendrites are distorted and likely nonstoichiometric with face-centered cubic structured domains of Li metal. These fundamental insights on the LiH formation may pave the way for enhancing the cycle stability of lithium batteries.Lithium hydride is a common but unfavorable component that leads to "dead Li" formation in lithium batteries. Since the hydrogen sources in the batteries are diverse and hardly evitable, unraveling the key factors promoting LiH formation is fundamentally crucial in improving lithium batteries' cycling stability. Herein, by using in situ environmental transmission electron microscope, we revealed a critical role of lithium fluoride in the LiH formation during the electrochemical deposition of Li in a hydrogen environment, presumably by facilitating the kinetic process of hydrogen dissociation and the LiH nucleation. Ex situ coin-cell studies and DFT calculations corroborate this finding, further suggesting that the commonly used fluorine-rich electrolytes could promote LiH formation. Additionally, the LiH lattices in the dendrites are distorted and likely nonstoichiometric with face-centered cubic structured domains of Li metal. These fundamental insights on the LiH formation may pave the way for enhancing the cycle stability of lithium batteries. Lithium hydride is a common but unfavorable component that leads to “dead Li” formation in lithium batteries. Since the hydrogen sources in the batteries are diverse and hardly evitable, unraveling the key factors promoting LiH formation is fundamentally crucial in improving lithium batteries’ cycling stability. Herein, by using in situ environmental transmission electron microscope, we revealed a critical role of lithium fluoride in the LiH formation during the electrochemical deposition of Li in a hydrogen environment, presumably by facilitating the kinetic process of hydrogen dissociation and the LiH nucleation. Ex situ coin-cell studies and DFT calculations corroborate this finding, further suggesting that the commonly used fluorine-rich electrolytes could promote LiH formation. Additionally, the LiH lattices in the dendrites are distorted and likely nonstoichiometric with face-centered cubic structured domains of Li metal. These fundamental insights on the LiH formation may pave the way for enhancing the cycle stability of lithium batteries. |
| Author | Hua, Ze Wang, Dazhuang Qiao, Lijie Ma, Yuan Ruan, Digen Zheng, Xuzhi Kang, Zhuo Yu, Xinyang Shao, Ruiwen Ren, Xiaodi He, Yang |
| AuthorAffiliation | University of Science and Technology of China University of Science and Technology Beijing Department of Materials Science and Engineering Academy for Advanced Interdisciplinary Science and Technology, State Key Laboratory for Advanced Metals and Materials Beijing Advanced Innovation Center for Materials Genome Engineering, School of Materials Science and Engineering Beijing Advanced Innovation Center for Intelligent Robots and Systems and School of Medical Technology |
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| Author_xml | – sequence: 1 givenname: Xinyang surname: Yu fullname: Yu, Xinyang organization: Beijing Advanced Innovation Center for Materials Genome Engineering, School of Materials Science and Engineering – sequence: 2 givenname: Digen surname: Ruan fullname: Ruan, Digen organization: University of Science and Technology of China – sequence: 3 givenname: Yuan surname: Ma fullname: Ma, Yuan organization: Beijing Advanced Innovation Center for Materials Genome Engineering, School of Materials Science and Engineering – sequence: 4 givenname: Xuzhi surname: Zheng fullname: Zheng, Xuzhi organization: University of Science and Technology Beijing – sequence: 5 givenname: Ze surname: Hua fullname: Hua, Ze organization: Beijing Advanced Innovation Center for Intelligent Robots and Systems and School of Medical Technology – sequence: 6 givenname: Ruiwen orcidid: 0000-0002-3082-0486 surname: Shao fullname: Shao, Ruiwen organization: Beijing Advanced Innovation Center for Intelligent Robots and Systems and School of Medical Technology – sequence: 7 givenname: Dazhuang surname: Wang fullname: Wang, Dazhuang organization: University of Science and Technology of China – sequence: 8 givenname: Zhuo surname: Kang fullname: Kang, Zhuo email: zhuokang@ustb.edu.cn organization: University of Science and Technology Beijing – sequence: 9 givenname: Xiaodi orcidid: 0000-0002-2025-7554 surname: Ren fullname: Ren, Xiaodi email: xdren@ustc.edu.cn organization: University of Science and Technology of China – sequence: 10 givenname: Lijie surname: Qiao fullname: Qiao, Lijie organization: Beijing Advanced Innovation Center for Materials Genome Engineering, School of Materials Science and Engineering – sequence: 11 givenname: Yang orcidid: 0000-0001-8095-2068 surname: He fullname: He, Yang email: yanghe@ustb.edu.cn organization: Beijing Advanced Innovation Center for Materials Genome Engineering, School of Materials Science and Engineering |
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| Keywords | lithium dendrite lithium fluoride lithium hydride solid-electrolyte interphase lithium battery |
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| Snippet | Lithium hydride is a common but unfavorable component that leads to “dead Li” formation in lithium batteries. Since the hydrogen sources in the batteries are... Lithium hydride is a common but unfavorable component that leads to "dead Li" formation in lithium batteries. Since the hydrogen sources in the batteries are... |
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| Title | In Situ Environmental Transmission Electron Microscopy Investigation on LiH Formation Prompted by LiF |
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