Constructions of a Set of New Lanthanide-Based Coordination Polymers with Hatza Ligands (Hatza = 5-Aminotetrazole−1-Acetic Acid)

Reaction of LnCl3·6H2O with 5-aminotetrazole-1-acetic acid (Hatza) under the presence of KOH produced a set of new Ln(III)/atza complexes, [Ln(atza)2(CH3OH)(H2O)Cl][Ln = Pr (1), Nd (2), Sm (3)], [Ln(atza)2 (H2O)3]Cl [Ln = Eu (4), Gd (5)], and [Tb(atza)2(H2O)4]Cl (6). These compounds were structurall...

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Published inCrystal growth & design Vol. 10; no. 1; pp. 165 - 170
Main Authors Li, Qiao-Yun, Yang, Gao-Wen, Tang, Xiao-Yan, Ma, Yun-Sheng, Yao, Wen, Zhou, Feng, Chen, Juan, Zhou, Hao
Format Journal Article
LanguageEnglish
Published Washington,DC American Chemical Society 06.01.2010
Subjects
Condensed matter: electronic structure, electrical, magnetic, and optical properties
Condensed matter: structure, mechanical and thermal properties
Exact sciences and technology
Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation
Optical properties of bulk materials and thin films
Physics
Structure of solids and liquids; crystallography
Structure of specific crystalline solids
Tetrazole derivatives
Molecular structure
Polychelate
Luminescence
Gadolinium
XRD
Rare earth complexes
Europium additions
Monocrystals
Rare earths
Optical properties
Ligands
Acetic acid
Europium
Crystal structure
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Abstract Reaction of LnCl3·6H2O with 5-aminotetrazole-1-acetic acid (Hatza) under the presence of KOH produced a set of new Ln(III)/atza complexes, [Ln(atza)2(CH3OH)(H2O)Cl][Ln = Pr (1), Nd (2), Sm (3)], [Ln(atza)2 (H2O)3]Cl [Ln = Eu (4), Gd (5)], and [Tb(atza)2(H2O)4]Cl (6). These compounds were structurally characterized by elemental analysis, IR spectroscopy, and single-crystal X-ray diffraction. The complexes 1−3 are isostructural and display two-dimensional frameworks, the isostructural complexes 4−5 show one-dimensional (1D) structures, and complex 6 forms a 1D framework. Furthermore, the luminescence properties of 4 and 6 were investigated at room temperature in the solid state.
AbstractList Reaction of LnCl3·6H2O with 5-aminotetrazole-1-acetic acid (Hatza) under the presence of KOH produced a set of new Ln(III)/atza complexes, [Ln(atza)2(CH3OH)(H2O)Cl][Ln = Pr (1), Nd (2), Sm (3)], [Ln(atza)2 (H2O)3]Cl [Ln = Eu (4), Gd (5)], and [Tb(atza)2(H2O)4]Cl (6). These compounds were structurally characterized by elemental analysis, IR spectroscopy, and single-crystal X-ray diffraction. The complexes 1−3 are isostructural and display two-dimensional frameworks, the isostructural complexes 4−5 show one-dimensional (1D) structures, and complex 6 forms a 1D framework. Furthermore, the luminescence properties of 4 and 6 were investigated at room temperature in the solid state.
Author Li, Qiao-Yun
Zhou, Hao
Zhou, Feng
Ma, Yun-Sheng
Yang, Gao-Wen
Tang, Xiao-Yan
Yao, Wen
Chen, Juan
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Issue 1
Keywords Tetrazole derivatives
Molecular structure
Polychelate
Luminescence
Gadolinium
XRD
Rare earth complexes
Europium additions
Monocrystals
Rare earths
Optical properties
Ligands
Acetic acid
Europium
Crystal structure
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Snippet Reaction of LnCl3·6H2O with 5-aminotetrazole-1-acetic acid (Hatza) under the presence of KOH produced a set of new Ln(III)/atza complexes,...
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SubjectTerms Condensed matter: electronic structure, electrical, magnetic, and optical properties
Condensed matter: structure, mechanical and thermal properties
Exact sciences and technology
Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation
Optical properties of bulk materials and thin films
Physics
Structure of solids and liquids; crystallography
Structure of specific crystalline solids
Title Constructions of a Set of New Lanthanide-Based Coordination Polymers with Hatza Ligands (Hatza = 5-Aminotetrazole−1-Acetic Acid)
URI http://dx.doi.org/10.1021/cg900807t
Volume 10
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