Influence of [Mo6Br8F6]2− Cluster Unit Inclusion within the Mesoporous Solid MIL-101 on Hydrogen Storage Performance

The inclusion of (TBA)2Mo6Br8F6 (TBA = tetrabutylammonium) containing [Mo6Br8F6]2− cluster units within the pores of the mesoporous chromium carboxylate MIL-101 (MIL stand for Materials from Institut Lavoisier) has been studied. X-ray powder diffraction, thermal analysis, elemental analysis, solid-s...

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Published inLangmuir Vol. 26; no. 13; pp. 11283 - 11290
Main Authors Dybtsev, Danil, Serre, Christian, Schmitz, Barbara, Panella, Barbara, Hirscher, Michael, Latroche, Michel, Llewellyn, Philip L, Cordier, Stéphane, Molard, Yann, Haouas, Mohamed, Taulelle, Francis, Férey, Gérard
Format Journal Article
LanguageEnglish
Published Washington, DC American Chemical Society 06.07.2010
Subjects
Chemical Sciences
Material chemistry
Materials: Nano-and Mesostructured Materials, Polymers, Gels, Liquid Crystals, Composites
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Abstract The inclusion of (TBA)2Mo6Br8F6 (TBA = tetrabutylammonium) containing [Mo6Br8F6]2− cluster units within the pores of the mesoporous chromium carboxylate MIL-101 (MIL stand for Materials from Institut Lavoisier) has been studied. X-ray powder diffraction, thermal analysis, elemental analysis, solid-state NMR, and infrared spectroscopy have evidenced the successful loading of the cluster. In a second step, the hydrogen sorption properties of the model cluster loaded metal organic framework (MOF) system have been analyzed and compared to those of the pure MOF sample, through a combination of adsorption isotherms (77 K, room temperature), thermal desorption spectroscopy, and calorimetry (calculated and experimental) in order to evaluate the hydrogen storage efficiency of the cluster loading.
AbstractList The inclusion of (TBA)(2)Mo(6)Br(8)F(6) (TBA = tetrabutylammonium) containing [Mo(6)Br(8)F(6)](2-) cluster units within the pores of the mesoporous chromium carboxylate MIL-101 (MIL stand for Materials from Institut Lavoisier) has been studied. X-ray powder diffraction, thermal analysis, elemental analysis, solid-state NMR, and infrared spectroscopy have evidenced the successful loading of the cluster. In a second step, the hydrogen sorption properties of the model cluster loaded metal organic framework (MOF) system have been analyzed and compared to those of the pure MOF sample, through a combination of adsorption isotherms (77 K, room temperature), thermal desorption spectroscopy, and calorimetry (calculated and experimental) in order to evaluate the hydrogen storage efficiency of the cluster loading.
The inclusion of (TBA)2Mo6Br8F6 (TBA = tetrabutylammonium) containing [Mo6Br8F6]2− cluster units within the pores of the mesoporous chromium carboxylate MIL-101 (MIL stand for Materials from Institut Lavoisier) has been studied. X-ray powder diffraction, thermal analysis, elemental analysis, solid-state NMR, and infrared spectroscopy have evidenced the successful loading of the cluster. In a second step, the hydrogen sorption properties of the model cluster loaded metal organic framework (MOF) system have been analyzed and compared to those of the pure MOF sample, through a combination of adsorption isotherms (77 K, room temperature), thermal desorption spectroscopy, and calorimetry (calculated and experimental) in order to evaluate the hydrogen storage efficiency of the cluster loading.
Author Llewellyn, Philip L
Panella, Barbara
Haouas, Mohamed
Férey, Gérard
Schmitz, Barbara
Dybtsev, Danil
Molard, Yann
Latroche, Michel
Taulelle, Francis
Serre, Christian
Hirscher, Michael
Cordier, Stéphane
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  fullname: Latroche, Michel
– sequence: 7
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Snippet The inclusion of (TBA)2Mo6Br8F6 (TBA = tetrabutylammonium) containing [Mo6Br8F6]2− cluster units within the pores of the mesoporous chromium carboxylate...
The inclusion of (TBA)(2)Mo(6)Br(8)F(6) (TBA = tetrabutylammonium) containing [Mo(6)Br(8)F(6)](2-) cluster units within the pores of the mesoporous chromium...
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SubjectTerms Chemical Sciences
Material chemistry
Materials: Nano-and Mesostructured Materials, Polymers, Gels, Liquid Crystals, Composites
Title Influence of [Mo6Br8F6]2− Cluster Unit Inclusion within the Mesoporous Solid MIL-101 on Hydrogen Storage Performance
URI http://dx.doi.org/10.1021/la100601a
https://www.ncbi.nlm.nih.gov/pubmed/20524701
https://hal.science/hal-00831632
Volume 26
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