Carbon Isotopic Ratios of Crude Oils by Stable Isotope Mass Spectrometry
To know about characteristics of crude oils with mass spectrometer, the carbon isotopic ratios measurements of 86 samples of crude oil from foreign and domestic fields were carried out. A quartz tube was used as a combustion vessel and vanadium pentoxide as an oxidation agent. A mixture of crude oil...
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| Published in | Journal of the Japanese Association for Petroleum Technology Vol. 54; no. 2; pp. 107 - 110 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English Japanese |
| Published |
The Japanese Association for Petroleum Technology
1989
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| Online Access | Get full text |
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| Abstract | To know about characteristics of crude oils with mass spectrometer, the carbon isotopic ratios measurements of 86 samples of crude oil from foreign and domestic fields were carried out. A quartz tube was used as a combustion vessel and vanadium pentoxide as an oxidation agent. A mixture of crude oil and vanadium pentoxide placed in the quartz tube was vacuumed and then sealed. This was heated for 2 hours at 900°C in electric furnace. Produced carbon dioxide was introduced to mass spectrometer to determine isotopic ratio. Foreign oil samples showed -27.7--22.0‰, as δ13C values. Results of domestic crude oils showed -24.0--24.1‰ in Hokkaidou, -24.5--21.9‰ in Akita, -23.7--21.7‰ in Yamagata, and -24.8--21.3‰ in Niigata, as δ13C values, which agreed well with the results of the Tertiary period oil in North America. |
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| AbstractList | To know about characteristics of crude oils with mass spectrometer, the carbon isotopic ratios measurements of 86 samples of crude oil from foreign and domestic fields were carried out. A quartz tube was used as a combustion vessel and vanadium pentoxide as an oxidation agent. A mixture of crude oil and vanadium pentoxide placed in the quartz tube was vacuumed and then sealed. This was heated for 2 hours at 900°C in electric furnace. Produced carbon dioxide was introduced to mass spectrometer to determine isotopic ratio. Foreign oil samples showed -27.7--22.0‰, as δ13C values. Results of domestic crude oils showed -24.0--24.1‰ in Hokkaidou, -24.5--21.9‰ in Akita, -23.7--21.7‰ in Yamagata, and -24.8--21.3‰ in Niigata, as δ13C values, which agreed well with the results of the Tertiary period oil in North America. |
| Author | TEZUKA, Machiko TANAKA, Shigeyuki OKADA, Shizuko |
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| References | 4) 関口嘉一•重川 守•平井明夫•宮本泰行, 1984: 地化学的見地から見た長岡•柏崎地域のグリーンタフ油•ガス鉱床の形成. 石技誌, 49, 57-64. 1) Des MARAIS D. J. and HAVES J. M., 1976: Tubu Cracker for Opening Glass-Sealed Ampoules under Vacuum. Anal. Chem., 48, 1651-1652. 2) SOFER Z., 1980: Preparation of Carbon Dioxide for Stable Isotope Analysis of Petroleum. Anal. Chem., 52, 1389-1391. 3) 重川 守, 1980: 原油と根源岩の対比. 石技誌, 45, 405-409. 6) 岡田静子•手塚真知子, 1989: 天然ガスおよびカッティングスガスの炭素同位体比測定における誤差要因の検計. (本誌 5) 安藤直行, 1974: 秋田•新潟地方産原油類の炭素同位体組成の概要. 石技誌, 39, 28-32. 7) DEGENS E. T, 1969: EGLINTON Edt. Organic Geochemistry chap. 12, 304. |
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| Title | Carbon Isotopic Ratios of Crude Oils by Stable Isotope Mass Spectrometry |
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