Design of Coupons and Test Methodology for Orthotropic Characterization of FFF-Processed Ultem 9085

The increasing prevalence of additive manufacturing (AM) methods such as fused filament fabrication (FFF) is motivating the need to reliably predict mechanical behavior of additively manufactured parts. However, predicting mechanical behavior is highly dependent on the availability of accurate prope...

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Published inStructural Integrity of Additive Manufactured Materials and Parts pp. 176 - 187
Main Authors Hyatt, Tommy, Martin, Richard, Fields, Rich
Format Book Chapter
LanguageEnglish
Published 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959 ASTM International 01.09.2020
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ISBN9780803177086
0803177089
DOI10.1520/STP163120190126

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Abstract The increasing prevalence of additive manufacturing (AM) methods such as fused filament fabrication (FFF) is motivating the need to reliably predict mechanical behavior of additively manufactured parts. However, predicting mechanical behavior is highly dependent on the availability of accurate property data. Recently published material property data for polyetherimide (PEI, or Ultem) provides a significant step toward quantifying AM process repeatability, but mechanical properties reported are specific to the geometry of the coupons and are therefore less useful for structural analysis of other geometries. In order to quantify material properties in a way that is generically applicable and scalable to any geometry within a finite element model, mechanical testing needs to account for the orthotropy inherent to the additive manufacturing process. Additionally, edge effects and differing extrusion directions that typically exist between the perimeter contour passes and the interior fill passes for each printed layer need to be considered and accounted for. Current industry best practices for coupon fabrication for tensile, compression, and shear were evaluated, tested, and iteratively modified to determine the most effective coupon design and test configurations for capturing the orthotropic properties of FFF-processed Ultem 9085. Using the improved coupon design and test methodologies, three sets of coupons were fabricated and tested for tensile, compression, and shear in X, Y, and Z directions—both for pure contour construction and also for pure raster construction. Mechanical property results demonstrate typical properties that are meaningfully different than currently published data. Typical property results are presented. Using orthotropic design allowables in finite element models will allow analysts to predict mechanical behavior of arbitrary AM geometry.
AbstractList The increasing prevalence of additive manufacturing (AM) methods such as fused filament fabrication (FFF) is motivating the need to reliably predict mechanical behavior of additively manufactured parts. However, predicting mechanical behavior is highly dependent on the availability of accurate property data. Recently published material property data for polyetherimide (PEI, or Ultem) provides a significant step toward quantifying AM process repeatability, but mechanical properties reported are specific to the geometry of the coupons and are therefore less useful for structural analysis of other geometries. In order to quantify material properties in a way that is generically applicable and scalable to any geometry within a finite element model, mechanical testing needs to account for the orthotropy inherent to the additive manufacturing process. Additionally, edge effects and differing extrusion directions that typically exist between the perimeter contour passes and the interior fill passes for each printed layer need to be considered and accounted for. Current industry best practices for coupon fabrication for tensile, compression, and shear were evaluated, tested, and iteratively modified to determine the most effective coupon design and test configurations for capturing the orthotropic properties of FFF-processed Ultem 9085. Using the improved coupon design and test methodologies, three sets of coupons were fabricated and tested for tensile, compression, and shear in X, Y, and Z directions—both for pure contour construction and also for pure raster construction. Mechanical property results demonstrate typical properties that are meaningfully different than currently published data. Typical property results are presented. Using orthotropic design allowables in finite element models will allow analysts to predict mechanical behavior of arbitrary AM geometry.
Author Hyatt, Tommy
Martin, Richard
Fields, Rich
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Copyright All rights reserved. This material may not be reproduced or copied, in whole or part, in any printed, mechanical, electronic, film, or other distribution and storage media, without the written consent of the publisher. 2020 ASTM International
2020
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Notes 2019-10-07 - 2019-10-10Fourth ASTM Symposium on Structural Integrity of Additive Manufactured Materials and PartsFort Washington, MD
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References Standard Test Method for Tensile Properties of Plastics, ASTM D638-14 (West Conshohocken, PA: ASTM International, approved December 15, 2014), https://doi.org/10.1520/D0638-14
OplingerD. W. , GandhiK. R. , and ParkerB. S. , Studies of Tension Test Specimens for Composite Material Testing, No. AMMRC-TR-82-27 (Watertown, MA: Army Materials and Mechanics Research Center, 1982).
Standard Test Method for Through-Thickness “Flatwise” Tensile Strength and Elastic Modulus of a Fiber-Reinforced Polymer Matrix Composite, ASTM D7291/D729M-07 (West Conshohocken, PA: ASTM International, approved April 1, 2007), https://doi.org/10.1520/D7291_D7291M-07
U.S. Department of Defense, “Guidelines for Property Testing of Composites,” in The Composite Materials Handbook, CMH-17, Vol. 1 (Washington, DC: 2002), 2.1–2.92.
Standard Test Methods for Tension Testing of Metallic Materials, ASTM E8/E8M-16a (West Conshohocken, PA: ASTM International, approved August 1, 2016), https://doi.org/10.1520/E0008_E0008M-16a
“America Makes Announces Complete, Qualified Database of Material Properties for Fused Deposition Modeling® (FDM®) Additive Manufacturing of ULTEM™ 9085 Resin,” America Makes, February 6, 2019, http://web.archive.org/web/20191031161905/https:/www.americamakes.us/america-makes-announces-complete-qualified-database-material-properties-fused-deposition-modeling-fdm-additive-manufacturing-ultem-9085-resin
Standard Test Method for Compressive Properties of Rigid Plastics, ASTM D695-15 (West Conshohocken, PA: ASTM International, approved September 1, 2015), https://doi.org/10.1520/D0695-15
Standard Test Method for Shear Properties of Composite Materials by the V-Notched Beam Method, ASTM D5379/D5379M-12 (West Conshohocken, PA: ASTM International, approved July 12, 2012), https://doi.org/10.1520/D5379_D5379M-12
References_xml – reference: Standard Test Method for Shear Properties of Composite Materials by the V-Notched Beam Method, ASTM D5379/D5379M-12 (West Conshohocken, PA: ASTM International, approved July 12, 2012), https://doi.org/10.1520/D5379_D5379M-12
– reference: “America Makes Announces Complete, Qualified Database of Material Properties for Fused Deposition Modeling® (FDM®) Additive Manufacturing of ULTEM™ 9085 Resin,” America Makes, February 6, 2019, http://web.archive.org/web/20191031161905/https:/www.americamakes.us/america-makes-announces-complete-qualified-database-material-properties-fused-deposition-modeling-fdm-additive-manufacturing-ultem-9085-resin
– reference: U.S. Department of Defense, “Guidelines for Property Testing of Composites,” in The Composite Materials Handbook, CMH-17, Vol. 1 (Washington, DC: 2002), 2.1–2.92.
– reference: Standard Test Method for Through-Thickness “Flatwise” Tensile Strength and Elastic Modulus of a Fiber-Reinforced Polymer Matrix Composite, ASTM D7291/D729M-07 (West Conshohocken, PA: ASTM International, approved April 1, 2007), https://doi.org/10.1520/D7291_D7291M-07
– reference: Standard Test Method for Tensile Properties of Plastics, ASTM D638-14 (West Conshohocken, PA: ASTM International, approved December 15, 2014), https://doi.org/10.1520/D0638-14
– reference: OplingerD. W. , GandhiK. R. , and ParkerB. S. , Studies of Tension Test Specimens for Composite Material Testing, No. AMMRC-TR-82-27 (Watertown, MA: Army Materials and Mechanics Research Center, 1982).
– reference: Standard Test Method for Compressive Properties of Rigid Plastics, ASTM D695-15 (West Conshohocken, PA: ASTM International, approved September 1, 2015), https://doi.org/10.1520/D0695-15
– reference: Standard Test Methods for Tension Testing of Metallic Materials, ASTM E8/E8M-16a (West Conshohocken, PA: ASTM International, approved August 1, 2016), https://doi.org/10.1520/E0008_E0008M-16a
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Snippet The increasing prevalence of additive manufacturing (AM) methods such as fused filament fabrication (FFF) is motivating the need to reliably predict mechanical...
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astm
SourceType Publisher
Enrichment Source
StartPage 176
SubjectTerms B-Basis
Characterization
Coupon Design
Fdm
Fff
Manufacturing Engineering
Materials & Manufacturing Processes
Orthotropy
Pei
Ultem
TableOfContents 12.1 Introduction 12.2 Manufacturing Repeatability 12.3 Mechanical Properties 12.4 FFF Construction Techniques 12.5 Orthotropy 12.6 Project Summary 12.7 Coupon Design-Pathfinding 12.8 Dimensional Inspection and Mechanical Testing 12.9 Minimum Test Matrix Size for Statistical Evaluation 12.10 Discussion of Results, Conclusions, and Future Work References
Title Design of Coupons and Test Methodology for Orthotropic Characterization of FFF-Processed Ultem 9085
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